2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

Base Information

Chemical Name:2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate
CAS No.:333954-48-6
Molecular Formula:C₂₇H₃₄ClNO₄SSi
Molecular Weight:532.176
Hs Code.:

Synonyms:2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

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Chemical Property of 2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

Chemical Property:

Purity/Quality:

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Technology Process of 2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

There total 6 articles about 2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 333954-47-5
3-[[tert-butyl(diphenyl)silyl]oxy]-2-(R)-(5-chloro-2-nitrobenzyl)propyl methanesulfonate

: 333954-48-6
2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

Guidance literature:: With acetic acid; In tetrahydrofuran;

Reference yield:

: 333954-33-9
2-(5-chloro-2-nitrobenzyl)propane-1,3-diol

: 333954-48-6
2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: lipase

2: water; N,N-dimethyl-formamide

3: potassium carbonate / methanol; water

4: sodium bicarbonate; triethylamine / acetonitrile

5: acetic acid / tetrahydrofuran

With sodium bicarbonate; potassium carbonate; acetic acid; triethylamine; lipase; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 333954-45-3
3-[[tert-butyl(diphenyl)silyl]oxy]-2-(S)-(5-chloro-2-nitrobenzyl)propyl propionate

: 333954-48-6
2-(R)-(2-amino-5-chlorobenzyl)-3-[[tert-butyl(diphenyl)silyl]oxy]propyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol; water

2: sodium bicarbonate; triethylamine / acetonitrile

3: acetic acid / tetrahydrofuran

With sodium bicarbonate; potassium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; water; acetonitrile;