N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

Base Information

Chemical Name:N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide
CAS No.:1287792-57-7
Molecular Formula:C₂₄H₂₀N₆O₅S₂
Molecular Weight:536.592
Hs Code.:

Synonyms:N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

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Chemical Property of N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

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Technology Process of N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

There total 4 articles about N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 3144-09-0
methanesulfonamide

: 1287792-54-4
7-(4-methanesulfonylaminophenyl)-2-phenyl-2H[1,2,3]triazolo[4,5-f]quinoline-9-carboxylic acid

: 1287792-57-7
N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

Guidance literature:: 7-(4-methanesulfonylaminophenyl)-2-phenyl-2H[1,2,3]triazolo[4,5-f]quinoline-9-carboxylic acid; With 1,1'-carbonyldiimidazole; In 1,2-dimethoxyethane; at 20 ℃; for 1h;

methanesulfonamide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,2-dimethoxyethane; at 60 ℃; for 1h;

Reference yield:

: 1287792-52-2
7-chloro-2-phenyl-2H[1,2,3]triazolo[4,5-f]quinoline-9-carboxylic acid methyl ester

: 1287792-57-7
N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 4 h / Inert atmosphere; Reflux

2.1: sodium hydroxide; water / acetonitrile / 3.5 h / Reflux

3.1: 1,1'-carbonyldiimidazole / 1,2-dimethoxyethane / 1 h / 20 °C

3.2: 1 h / 60 °C

With water; caesium carbonate; 1,1'-carbonyldiimidazole; sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 616880-14-9
N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanesulfonamide

: 1287792-57-7
N-[7-(4-methanesulfonylaminophenyl)-2-phenyl-2H-[1,2,3]-triazolo[4,5-f]quinoline-9-carbonyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 4 h / Inert atmosphere; Reflux

2.1: sodium hydroxide; water / acetonitrile / 3.5 h / Reflux

3.1: 1,1'-carbonyldiimidazole / 1,2-dimethoxyethane / 1 h / 20 °C

3.2: 1 h / 60 °C

With water; caesium carbonate; 1,1'-carbonyldiimidazole; sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile;