C₅₄H₆₆N₄O₉

Base Information

Chemical Name:C₅₄H₆₆N₄O₉
CAS No.:362517-28-0
Molecular Formula:C₅₄H₆₆N₄O₉
Molecular Weight:915.139
Hs Code.:

C<sub>54</sub>H<sub>66</sub>N<sub>4</sub>O<sub>9</sub>

Synonyms:C₅₄H₆₆N₄O₉

Suppliers and Price of C₅₄H₆₆N₄O₉

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₆₆N₄O₉

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₆₆N₄O₉

There total 16 articles about C₅₄H₆₆N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: 362517-27-9
C₆₁H₇₄N₄O₁₂S

: 362517-28-0
C₅₄H₆₆N₄O₉

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; for 16h;
DOI:10.1021/jo000250y

Reference yield:

: 362517-11-1
(3aR,4S,5S,11bS)-methyl 2,3,3a,4,5,7-hexahydro-4-[(2S)-2-ethyl-2,3-(isopropylidenedioxy)propyl]-1H-pyrrolo[2,3-d]carbazole-5-hydroxymethyl-6-carboxylate

: 362517-28-0
C₅₄H₆₆N₄O₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

2.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

2.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

3.1: thiocresol / 2 h / 110 °C

3.2: tributyltin hydride; 2,2'-diazobisisobutyronitrile / toluene / 24 h / Heating

3.3: H₂; triethylamine / Pd(OH)2/C / ethyl acetate / 1 h

4.1: 1.231 g / triethylamine; potassium carbonate / acetone / 15 h

5.1: tert-butyl hypochlorite; triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

6.1: tetrafluoroboric acid-dimethyl ether copmlex; silver tetrafluoroborate / acetone / 1 h / -10 °C

7.1: potassium borohydride / acetic acid / 0.5 h / 0 °C

7.2: 1.183 g / aq. hydrochloric acid / methanol / 0.25 h / Heating

8.1: 54.3 percent / triethylamine / CH₂Cl₂ / 2 h

9.1: 93.6 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h

With dmap; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; p-toluenesulfonylanhydride; sodium hydrogencarbonate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; para-thiocresol; tetrafluoroboric acid dimethyl ether complex; In tetrahydrofuran; dichloromethane; water; acetic acid; acetone;
DOI:10.1021/jo000250y

Reference yield:

: 362517-06-4
(3aR,4S,5S,11bS)-dimethyl 3-benzyl-2,3,3a,4,5,7-hexahydro-4-[(2R)-2-ethyl-2,3-epoxypropyl]-1H-pyrrolo[2,3-d]carbazole-5,6-dicarboxylate

: 362517-28-0
C₅₄H₆₆N₄O₉

Guidance literature:: Multi-step reaction with 12 steps

1.1: 13.6 percent / sulfuric acid/silica gel; water / dioxane / 0.17 h

2.1: 81.7 percent / diisobutylaluminum hydride / tetrahydrofuran; hexane / 0 - 20 °C

3.1: ammonium formate / Pd/C / methanol; ethyl acetate / 2 h / Heating

4.1: 6.940 g / sodium hydrogencarbonate / acetone; H₂O / 0.33 h / 0 °C

5.1: p-toluenesulfonic anhydride; triethylamine; 4-dimethylaminopyridine / CH₂Cl₂ / 5 h

5.2: 92.3 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 24 h

6.1: thiocresol / 2 h / 110 °C

6.2: tributyltin hydride; 2,2'-diazobisisobutyronitrile / toluene / 24 h / Heating

6.3: H₂; triethylamine / Pd(OH)2/C / ethyl acetate / 1 h

7.1: 1.231 g / triethylamine; potassium carbonate / acetone / 15 h

8.1: tert-butyl hypochlorite; triethylamine / CH₂Cl₂ / 0.33 h / 0 °C

9.1: tetrafluoroboric acid-dimethyl ether copmlex; silver tetrafluoroborate / acetone / 1 h / -10 °C

10.1: potassium borohydride / acetic acid / 0.5 h / 0 °C

10.2: 1.183 g / aq. hydrochloric acid / methanol / 0.25 h / Heating

11.1: 54.3 percent / triethylamine / CH₂Cl₂ / 2 h

12.1: 93.6 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h

With dmap; silver tetrafluoroborate; potassium borohydride; tert-butylhypochlorite; sulfuric acid; p-toluenesulfonylanhydride; water; ammonium formate; silica gel; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; para-thiocresol; tetrafluoroboric acid dimethyl ether complex; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; acetic acid; ethyl acetate; acetone;
DOI:10.1021/jo000250y