tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

Base Information

Chemical Name:tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate
CAS No.:1313189-63-7
Molecular Formula:C₃₅H₃₈F₇NO₅S₂
Molecular Weight:749.811
Hs Code.:

tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

Synonyms:tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

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Chemical Property of tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

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Technology Process of tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

There total 10 articles about tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 559-40-0
octaperfluorocyclopentene

: 1313189-62-6
tert-butyl N-[2-(4-{4'-bromo-5'-methyl-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]-N-methylcarbamate

: C₃₀H₃₉NO₅S₂

: 1313189-63-7
tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

: 1313189-66-0
C₆₅H₇₆F₆N₂O₁₀S₄

Guidance literature:: tert-butyl N-[2-(4-{4'-bromo-5'-methyl-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]-N-methylcarbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

octaperfluorocyclopentene; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201100166

Reference yield:

: 111881-86-8
methyl 2-(2-bromothiophen-3-yl)ethan-1-ol

: C₃₀H₃₉NO₅S₂

: 1313189-63-7
tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

: 1313189-66-0
C₆₅H₇₆F₆N₂O₁₀S₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / diethyl ether / 4 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 - 20 °C / Inert atmosphere

3.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; hexane; water / 18 h / 78 °C / Inert atmosphere

4.1: iodine; mercury(II) oxide / benzene / 20 °C / Inert atmosphere

5.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; hexane; water / 24 h / 78 °C / Inert atmosphere

6.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

6.2: 1 h / -78 °C / Inert atmosphere

With n-butyllithium; iodine; sodium carbonate; toluene-4-sulfonic acid; triphenylphosphine; mercury(II) oxide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; hexane; water; benzene; 3.1: Suzuki coupling / 5.1: Suzuki coupling;
DOI:10.1002/ejoc.201100166

Reference yield:

: 554-14-3
2-Methylthiophene

: C₃₀H₃₉NO₅S₂

: 1313189-63-7
tert-butyl N-methyl-N-[2-(4-{5'-methyl-4'-(heptafluorocyclopent-1-enyl)-4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl][2,2']bithiophen-5-yl}phenoxy)ethyl]carbamate

: 1313189-66-0
C₆₅H₇₆F₆N₂O₁₀S₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine; acetic acid / 12 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

2.3: Inert atmosphere

3.1: sodium carbonate; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; hexane; water / 24 h / 78 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

With n-butyllithium; bromine; sodium carbonate; acetic acid; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; hexane; water; 3.1: Suzuki coupling;
DOI:10.1002/ejoc.201100166