C₅₂H₆₆O₇Si₂

Base Information

Chemical Name:C₅₂H₆₆O₇Si₂
CAS No.:1018988-59-4
Molecular Formula:C₅₂H₆₆O₇Si₂
Molecular Weight:859.263
Hs Code.:

C<sub>52</sub>H<sub>66</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:C₅₂H₆₆O₇Si₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₆₆O₇Si₂

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of C₅₂H₆₆O₇Si₂

There total 1 articles about C₅₂H₆₆O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1018988-43-6
C₅₄H₆₈O₈Si₂

: 1018988-59-4
C₅₂H₆₆O₇Si₂

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1002/anie.200704959

Reference yield: 97.0%

: 1018988-59-4
C₅₂H₆₆O₇Si₂

: 1018988-44-7
C₅₂H₆₈O₇Si₂

Guidance literature:: With sodium tetrahydroborate; In ethanol; at -78 ℃; for 2h;
DOI:10.1002/anie.200704959

Reference yield:

: 1018988-59-4
C₅₂H₆₆O₇Si₂

: 1192365-17-5
C₄₄H₆₂O₆Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / ethanol / 2 h / -78 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 39 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 13 °C / Inert atmosphere

7.1: lithium borohydride / tetrahydrofuran / Inert atmosphere; Reflux

7.2: 4 h / 20 °C / Inert atmosphere

8.1: lithium borohydride / tetrahydrofuran / 26.5 h / 20 °C / Inert atmosphere; Reflux

8.2: 4 h / 20 °C / Inert atmosphere

9.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

9.2: 20 °C / Inert atmosphere

With sodium tetrahydroborate; lithium borohydride; 2,6-di-tert-butyl-4-methylpyridine; water; sodium hydrogencarbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile; 5.1: Luche reduction;
DOI:10.1002/asia.200800429