tert-butyl 4-iodocinnamate

Base Information

Chemical Name:tert-butyl 4-iodocinnamate
CAS No.:162936-34-7
Molecular Formula:C₁₃H₁₅IO₂
Molecular Weight:330.165
Hs Code.:

Synonyms:tert-butyl 4-iodocinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 4-iodocinnamate

Chemical Property:

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Technology Process of tert-butyl 4-iodocinnamate

There total 1 articles about tert-butyl 4-iodocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 162936-33-6
4-aminocinnamic acid tert-butyl ester

: 162936-34-7
tert-butyl 4-iodocinnamate

Guidance literature:: With diiodomethane; isopentyl nitrite; at 85 ℃; for 0.5h;
DOI:10.1021/jm00009a007

Reference yield:

: 162936-34-7
tert-butyl 4-iodocinnamate

: (E)-3-(4-Trimethylsilanylethynyl-phenyl)-acrylic acid tert-butyl ester

: tert-butyl 3-(4-ethynylphenyl)acrylate

Guidance literature:: With potassium hydroxide; In methanol; for 0.5h; Yield given; Ambient temperature;
DOI:10.1021/jm00009a007

Reference yield:

: 162936-34-7
tert-butyl 4-iodocinnamate

: 1066-54-2
trimethylsilylacetylene

: (E)-3-(4-Trimethylsilanylethynyl-phenyl)-acrylic acid tert-butyl ester

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In acetonitrile; for 24h;
DOI:10.1021/jm00009a007