penta-O-benzoyl-5-fluoro-β-D-glucopyranose

Base Information

• Chemical Name: penta-O-benzoyl-5-fluoro-β-D-glucopyranose
• CAS No.: 753492-14-7
• Molecular Formula: C₄₁H₃₁FO₁₁
• Molecular Weight: 718.689
• Mol file: 753492-14-7.mol

Synonyms:penta-O-benzoyl-5-fluoro-β-D-glucopyranose

Chemical Property of penta-O-benzoyl-5-fluoro-β-D-glucopyranose

Chemical Property:

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Technology Process of penta-O-benzoyl-5-fluoro-β-D-glucopyranose

There total 1 articles about penta-O-benzoyl-5-fluoro-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1,2,3,4,6-penta-O-benzoyl-5-C-bromo-β-D-glucopyranose (69534-63-0) → C41H31FO11 + penta-O-benzoyl-5-fluoro-β-D-glucopyranose (753492-14-7)

Guidance literature:

With silver tetrafluoroborate; In diethyl ether; dichloromethane;

DOI:10.1071/CH03288

Reference yield: 78.0%

penta-O-benzoyl-5-fluoro-β-D-glucopyranose (753492-14-7) → 1,2,3,4,6-penta-O-benzoyl-5-C-bromo-β-D-glucopyranose (69534-63-0)

Guidance literature:

With hydrogen bromide; acetic acid; at 20 ℃; for 72h;

DOI:10.1071/CH03288

Reference yield:

penta-O-benzoyl-5-fluoro-β-D-glucopyranose (753492-14-7) → C41H31FO11

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / HBr; AcOH / 72 h / 20 °C

2: 8 percent / silver tetrafluoroborate / diethyl ether; CH₂Cl₂

With silver tetrafluoroborate; hydrogen bromide; acetic acid; In diethyl ether; dichloromethane;

DOI:10.1071/CH03288

upstream raw materials:

1,2,3,4,6-penta-O-benzoyl-5-C-bromo-β-D-glucopyranose

Downstream raw materials:

1,2,3,4,6-penta-O-benzoyl-5-C-bromo-β-D-glucopyranose