6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

Base Information

Chemical Name:6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one
CAS No.:1033586-60-5
Molecular Formula:C₂₂H₁₇BrCl₂N₂O₂
Molecular Weight:492.199
Hs Code.:

Synonyms:6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

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Chemical Property of 6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

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Technology Process of 6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

There total 3 articles about 6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1033586-59-2
6-(2-chloroacetyl)-2,2-dimethyl-2,3-dihydropyran-4-one

: 1033586-85-4
C₁₃H₉BrCl₂N₂

: 1033586-60-5
6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 80 - 85 ℃; for 24h;

Reference yield:

: 80866-93-9
3,4-dihydro-2,2-dimethyl-4-oxo-2H-pyran-6-carboxylic acid

: 1033586-60-5
6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 0 - 20 °C

2.1: tetrahydrofuran; acetonitrile / 3 h / 20 °C

2.2: 1 h / 20 °C

3.1: sodium hydrogencarbonate / tetrahydrofuran / 24 h / 80 - 85 °C

With oxalyl dichloride; sodium hydrogencarbonate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 137178-89-3
6,6-dimethyl-4-oxo-5,6-dihydro-4H-pyran-2-carbonyl chloride

: 1033586-60-5
6-[1-(4-bromo-2-chlorophenyl)-2-(2-chlorophenyl)-1H-imidazol-4-yl]-2,2-dimethyl-2,3-dihydropyran-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; acetonitrile / 3 h / 20 °C

1.2: 1 h / 20 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran / 24 h / 80 - 85 °C

With sodium hydrogencarbonate; In tetrahydrofuran; acetonitrile;