1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

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Chemical Name:1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene
CAS No.:1534391-69-9
Molecular Formula:C₆₂H₉₂O₆
Molecular Weight:933.409
Hs Code.:

Synonyms:1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

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Chemical Property of 1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

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Technology Process of 1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

There total 9 articles about 1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1534391-67-7
{1-[3,4-bis(hexyloxy)naphthalen-2-yl]methylidene}phenylamine

: 1534391-65-5
1-{(E)-2-[2,3-bis(hexyloxy)phenyl]vinyl}-2,3-bis(hexyloxy)-4-methylbenzene

: 1534391-69-9
1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 - 90 ℃; for 2h;
DOI:10.5560/ZNB.2013-3170

Reference yield:

: 111-25-1
1-bromo-hexane

: 1534391-69-9
1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate; potassium iodide / acetone / 72 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 2 h / Reflux

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 12 h / 20 °C / Inert atmosphere

4: chloroform / 24 h / Reflux

5: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / 20 - 90 °C

With lithium aluminium tetrahydride; potassium tert-butylate; potassium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium iodide; In 1,4-dioxane; diethyl ether; chloroform; N,N-dimethyl-formamide; acetone; 5: |Siegrist Stilbene Synthesis;
DOI:10.5560/ZNB.2013-3170

Reference yield:

: 144412-81-7
2,3-bis(hexyloxy)-4-methylbenzaldehyde

: 1534391-69-9
1,2-bis(hexyloxy)-3-((E)-2-{2,3-bis(hexyloxy)-4-[(E)-2-(2,3-bis(hexyloxy)phenyl)vinyl]phenyl}vinyl)naphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / paraffin oil; 1,2-dimethoxyethane / 6 h / Inert atmosphere; Reflux

2: potassium tert-butylate / N,N-dimethyl-formamide / 2 h / 20 - 90 °C

With potassium tert-butylate; sodium hydride; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; paraffin oil; 1: |Wittig-Horner Reaction / 2: |Siegrist Stilbene Synthesis;
DOI:10.5560/ZNB.2013-3170