diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

Base Information

Chemical Name:diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate
CAS No.:939388-05-3
Molecular Formula:C₂₀H₂₈NO₅PS
Molecular Weight:425.486
Hs Code.:

Synonyms:diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

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Chemical Property of diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

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Technology Process of diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

There total 3 articles about diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 942631-72-3
diethyl (Z)-3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)prop-1-enylphosphonate

: 939388-05-3
diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

Guidance literature:: With hydrogen; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 4h; atmospheric pressure;
DOI:10.1021/jo0700981

Reference yield: 65.0%

: 939388-05-3
diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

Guidance literature:

Reference yield:

: 939387-57-2
diethyl (E)-3-[N-acetyl-N-(benzyloxy)amino]-1-(tributylstannyl)prop-1-enylphosphonate

: 939388-05-3
diethyl 3-[N-acetyl-N-(benzyloxy)amino]-1-(thien-3-yl)propylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / (2-furyl)3P; CuI / Pd₂dba3*CHCl₃ / 1-methyl-pyrrolidin-2-one / 20 °C

2: 65 percent / H₂; Na₂CO₃ / Pd/C / tetrahydrofuran / 4 h / 20 °C / atmospheric pressure

With copper(l) iodide; trifuran-2-yl-phosphane; hydrogen; sodium carbonate; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; palladium on activated charcoal; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; 1: Stille coupling;
DOI:10.1021/jo0700981