1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

Base Information

Chemical Name:1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside
CAS No.:1448686-59-6
Molecular Formula:C₄₅H₇₈O₁₂Si
Molecular Weight:839.193
Hs Code.:

1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

Synonyms:1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

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Chemical Property of 1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

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Technology Process of 1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

There total 1 articles about 1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1448686-58-5
1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 1448686-59-6
1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

Guidance literature:: With water; potassium hydroxide; In tetrahydrofuran; at 55 ℃; for 6h;
DOI:10.1021/ol4020255

Reference yield: 92.0%

: 1448686-59-6
1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 1448686-60-9
C₄₅H₇₆O₁₁Si

Guidance literature:: With dmap; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; In 1,2-dichloro-ethane; for 3h; Reagent/catalyst; Solvent; Temperature; Time; Reflux;
DOI:10.1021/ol4020255

Reference yield:

: 1448686-59-6
1-(hydroxycarbonyl)pentadec-10(S)-yl 3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 1448686-61-0
C₃₉H₆₂O₁₁

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide; dmap; pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 3 h / Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 48 h / 30 °C

With dmap; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ol4020255