2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

Base Information

Chemical Name:2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone
CAS No.:853996-34-6
Molecular Formula:C₁₉H₂₉O₁₀P
Molecular Weight:448.407
Hs Code.:

Synonyms:2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

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Technology Process of 2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

There total 5 articles about 2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 853996-33-5
2,3-di-O-benzoyl-5-deoxy-5-diphenylphosphate-D-ribono-1,4-lactone

: 853996-34-6
2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

Guidance literature:: With hydrogen; platinum(IV) oxide; In dichloromethane; for 144h; under 18751.5 Torr;
DOI:10.1016/j.tetlet.2005.03.151

Reference yield:

: 853996-32-4
2,3-di-O-benzoyl-D-ribono-1,4-lactone

: 853996-34-6
2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / 15 h / 25 °C

2: 100 percent / H₂ / PtO₂ / CH₂Cl₂ / 144 h / 18751.5 Torr

With pyridine; hydrogen; platinum(IV) oxide; In dichloromethane;
DOI:10.1016/j.tetlet.2005.03.151

Reference yield:

: 853996-31-3
2,3-di-O-benzoyl-5-O-triphenylmethyl-D-ribono-1,4-lactone

: 853996-34-6
2,3-di-O-cyclohexanoyl-5-deoxy-5-dihydrogenophosphate-D-ribono-1,4-lactone

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂ / Pd/C / CH₂Cl₂ / 144 h / 25 °C / 11250.9 Torr

2: 95 percent / pyridine / 15 h / 25 °C

3: 100 percent / H₂ / PtO₂ / CH₂Cl₂ / 144 h / 18751.5 Torr

With pyridine; hydrogen; platinum(IV) oxide; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/j.tetlet.2005.03.151