Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium;

Base Information

• Chemical Name: Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium
• CAS No.: 84202-28-8
• Molecular Formula: CF₃O₃S*C₂₉H₂₈N
• Molecular Weight: 539.618

Synonyms:Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium;

Chemical Property of Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium;

Chemical Property:

Purity/Quality:

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Technology Process of Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium;

There total 3 articles about Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-phenyl-4-(p-tolyl)-5,6,7,8-tetrahydrochromenylium triflate (84202-11-9) + benzylamine (100-46-9) → Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium; (84202-28-8)

Guidance literature:

In dichloromethane; at 25 ℃; for 4h;

DOI:10.1016/0040-4020(82)85086-2

Reference yield:

4-methyl-chalcone (4224-87-7) → Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium; (84202-28-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / diethyl ether / 2 h / Ambient temperature

2: 97 percent / CH₂Cl₂ / 4 h / 25 °C

In diethyl ether; dichloromethane;

DOI:10.1016/0040-4020(82)85086-2

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → Trifluoro-methanesulfonate1-benzyl-2-phenyl-4-p-tolyl-5,6,7,8-tetrahydro-quinolinium; (84202-28-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / diethyl ether / 2 h / Ambient temperature

2: 97 percent / CH₂Cl₂ / 4 h / 25 °C

In diethyl ether; dichloromethane;

DOI:10.1016/0040-4020(82)85086-2

upstream raw materials:

2-phenyl-4-(p-tolyl)-5,6,7,8-tetrahydrochromenylium triflate

benzylamine

4-methyl-chalcone

cyclohexanone

Downstream raw materials:

1-Benzyl-2-phenyl-4-p-tolyl-1,5,6,7-tetrahydro-quinoline

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