ethyl 12-(3-nitrophenyl)-11-dodecenoate

Base Information

Chemical Name:ethyl 12-(3-nitrophenyl)-11-dodecenoate
CAS No.:102831-65-2
Molecular Formula:C₂₀H₂₉NO₄
Molecular Weight:347.455
Hs Code.:

Synonyms:ethyl 12-(3-nitrophenyl)-11-dodecenoate

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Chemical Property of ethyl 12-(3-nitrophenyl)-11-dodecenoate

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Technology Process of ethyl 12-(3-nitrophenyl)-11-dodecenoate

There total 1 articles about ethyl 12-(3-nitrophenyl)-11-dodecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 99-61-6
3-nitro-benzaldehyde

: 102831-64-1
(11-carbethoxyundecyl)triphenylphosphonium bromide

: 102831-65-2
ethyl 12-(3-nitrophenyl)-11-dodecenoate

Guidance literature:: With sodium amide; In tetrahydrofuran; for 4.5h;
DOI:10.1021/jm00129a020

Reference yield: 97.5%

: 102831-65-2
ethyl 12-(3-nitrophenyl)-11-dodecenoate

: 102831-67-4
ethyl 12-(3-aminophenyl)dodecanoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h; under 2327.2 Torr; Ambient temperature;
DOI:10.1021/jm00129a020

Reference yield:

: 102831-65-2
ethyl 12-(3-nitrophenyl)-11-dodecenoate

: 121269-37-2
12-(m-iodophenyl)dodecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 97.5 percent / H₂ / 5percent Pd/C / ethyl acetate / 4 h / 2327.2 Torr / Ambient temperature

2: 1) glacial acetic acid, conc. HCl, NaNO₂, 2) KI, I₂ / 1) H₂O, 40 min, 0 deg C, 2) overnight, r.t.

3: 88 percent / KOH / aq. ethanol / Heating

With hydrogenchloride; potassium hydroxide; hydrogen; iodine; acetic acid; potassium iodide; sodium nitrite; palladium on activated charcoal; In ethanol; ethyl acetate;
DOI:10.1021/jm00129a020