Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

Base Information

Chemical Name:Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate
CAS No.:84708-56-5
Molecular Formula:C₂₄H₃₃NO₉
Molecular Weight:479.527
Hs Code.:

Synonyms:Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

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Chemical Property of Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

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Technology Process of Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

There total 4 articles about Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 42854-62-6
L-alanine benzyl ester p-toluenesulfonate

: 84708-54-3
[(3aR,5R,6S,6aR)-5-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yloxy]-acetic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 84708-56-5
Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

Guidance literature:: With triethylamine; for 48h; Ambient temperature;

Reference yield:

: 350255-13-9
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 84708-56-5
Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / NaH / tetrahydrofuran / 6 h / 0 °C

2: 100 percent / 1 N NaOH / 1 h / Heating

3: tetrahydrofuran / 1) ice bath, 3 h, 2) r.t., 1 h

4: 50 percent / Et₃N / 48 h / Ambient temperature

With sodium hydroxide; sodium hydride; triethylamine; In tetrahydrofuran;

Reference yield:

: 64697-82-1
(-)-1,2:5,6-Di-O-isopropylidene-3-O-carboxymethyl-α-D-glucofuranose

: 84708-56-5
Benzyl N-<(1,2:5,6-Di-O-isopropylidene-α-D-glucofuranos-3-O-yl)acetyl>-L-alaninate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1) ice bath, 3 h, 2) r.t., 1 h

2: 50 percent / Et₃N / 48 h / Ambient temperature

With triethylamine; In tetrahydrofuran;