N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

Base Information

Chemical Name:N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide
CAS No.:1370347-36-6
Molecular Formula:C₁₇H₂₀ClN₅O₅S
Molecular Weight:441.895
Hs Code.:

Synonyms:N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

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Chemical Property of N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

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Technology Process of N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

There total 10 articles about N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 138229-58-0
phenyl 4-methoxypyrimidin-2-ylcarbamate

: 1370347-11-7
N-(4-chloro-3-sulfamoylphenyl)pivalamide

: 1370347-36-6
N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃;
DOI:10.1016/j.ejmech.2012.01.011

Reference yield:

: 2015-19-2
5-amino-2-chlorobenzenesulfonamide

: 1370347-36-6
N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.ejmech.2012.01.011

Reference yield:

: 155-90-8
4-methoxypyrimidin-2-amine

: 1370347-36-6
N-(4-chloro-3-(N-(4-methoxypyrimidin-2-ylcarbamoyl)sulfamoyl)phenyl)pivalamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetone; acetonitrile;
DOI:10.1016/j.ejmech.2012.01.011