2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

Base Information

Chemical Name:2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane
CAS No.:88328-23-8
Molecular Formula:C₂₆H₂₆N₄O₆
Molecular Weight:490.516
Hs Code.:

Synonyms:2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

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Chemical Property of 2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

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Technology Process of 2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

There total 3 articles about 2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 941-69-5
N-phenyl-maleimide

: 122908-64-9,82276-93-5
Schiff base pyridoxal-pyridoxamine

: 88328-23-8
2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

Guidance literature:: In acetonitrile; at 100 ℃; for 20h;
DOI:10.1016/S0040-4039(00)88342-2

Reference yield:

: 524-36-7
pyridoxamine dihydrochloride

: 88328-23-8
2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / potassium hydroxide / 0.5 h / Ambient temperature

2: 72 percent / acetonitrile / 20 h / 80 °C

With potassium hydroxide; In acetonitrile;
DOI:10.1016/S0040-4020(01)86100-7

Reference yield:

: 65-22-5
pyridoxal hydrochloride

: 88328-23-8
2,4-bis(3'-hydroxy-5'-hydroxymethyl-2'-methyl-4'-pyridyl)-7-phenyl-6,8-dioxo-3,7-diazabicyclo<3.3.0>octane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / potassium hydroxide / 0.5 h / Ambient temperature

2: 72 percent / acetonitrile / 20 h / 80 °C

With potassium hydroxide; In acetonitrile;
DOI:10.1016/S0040-4020(01)86100-7