((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

Base Information

Chemical Name:((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate
CAS No.:1352007-80-7
Molecular Formula:C₃₂H₃₃N₃O₃S
Molecular Weight:539.698
Hs Code.:

Synonyms:((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

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Chemical Property of ((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

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Technology Process of ((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

There total 5 articles about ((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1352007-90-9
(4R,5R)-4,5-diphenyl-1-(o-tolyl)imidazoline

: 823785-72-4
(4R,5R)-3,4-dimethyl-5-phenyl-1,2,3-oxathiazolidine-2,2-dioxide

: 1352007-80-7
((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

Guidance literature:: In dichloromethane; at 20 ℃; for 144h;
DOI:10.1016/j.tetasy.2011.09.018

Reference yield:

: 1352007-88-5
(1R,2R)-1,2-diphenyl-N₁-(o-tolyl)ethane-1,2-diamine

: 1352007-80-7
((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / acetonitrile / 1 h / Reflux; Inert atmosphere

2: dichloromethane / 144 h / 20 °C

With acetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetasy.2011.09.018

Reference yield:

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 1352007-80-7
((1S,2R)-1-((4R,5R)-4,5-diphenyl-1-(o-tolyl)-4,5-dihydro-1H-imidazol-3-ium-3-yl)-1-phenylpropan-2-yl)(methyl)sulfamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 16 h / 100 °C / Inert atmosphere

2: acetic acid / acetonitrile / 1 h / Reflux; Inert atmosphere

3: dichloromethane / 144 h / 20 °C

With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; acetic acid; sodium t-butanolate; In dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.tetasy.2011.09.018