C₃₂H₄₁N₅O₈

Base Information

Chemical Name:C₃₂H₄₁N₅O₈
CAS No.:1353660-92-0
Molecular Formula:C₃₂H₄₁N₅O₈
Molecular Weight:623.706
Hs Code.:

C<sub>32</sub>H<sub>41</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:C₃₂H₄₁N₅O₈

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Chemical Property of C₃₂H₄₁N₅O₈

Chemical Property:

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Technology Process of C₃₂H₄₁N₅O₈

There total 7 articles about C₃₂H₄₁N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 873326-27-3
(R)-2-((S)-2-((tert-butoxycarbonyl)amino)-N-methyl propanamido)-3-(1H-indol-3-yl)propanoic acid

: 1353660-61-3
C₁₂H₁₆N₂O₄

: 1353660-92-0
C₃₂H₄₁N₅O₈

Guidance literature:: With benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at -10 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201101978

Reference yield:

: 1353724-28-3
(2S,3R)-methyl 3-(4-cyanophenyl)-2,3-dihydroxypropanoate

: 1353660-92-0
C₃₂H₄₁N₅O₈

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen azide; triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / -25 - 20 °C / Inert atmosphere

2: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

3: dihydrogen peroxide; potassium carbonate / methanol; water / 2 h / 20 °C

4: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

5: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

With hydrogen azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1002/chem.201101978

Reference yield:

: 1353660-42-0
(2S,3S)-methyl 3-azido-3-(4-cyanophenyl)-2-hydroxypropanoate

: 1353660-92-0
C₃₂H₄₁N₅O₈

Guidance literature:: Multi-step reaction with 4 steps

1: proton sponge / 1,2-dichloro-ethane / 40 °C / Inert atmosphere

2: dihydrogen peroxide; potassium carbonate / methanol; water / 2 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

4: benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / -10 - 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; potassium carbonate; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In methanol; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101978