N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide

Base Information

• Chemical Name: N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide
• CAS No.: 1068148-11-7
• Molecular Formula: C₃₉H₄₇N₇O₇
• Molecular Weight: 725.845

Synonyms:N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide

Chemical Property of N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide

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Technology Process of N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide

There total 1 articles about N-(5-(2-(benzyl(6-(N₆-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

N-(5-(2-((6-aminohexyl)(benzyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide trifluoroacetate (1068148-09-3) + 6-Chloropurine riboside (2004-06-0) → N-(5-(2-(benzyl(6-(N6-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide (1068148-11-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tert-butyl alcohol; at 80 ℃; for 48h; Inert atmosphere;

DOI:10.1021/jm800613s

Reference yield: 5.0%

N-(5-(2-(benzyl(6-(N6-adenosinyl)hexyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide (1068148-11-7) → N-(2-hydroxy-5-(1-hydroxy-2-(6-(N6-adenosinyl)hexylamino)ethyl)phenyl)formamide (1068148-16-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; for 48h; under 2585.81 Torr;

DOI:10.1021/jm800613s

upstream raw materials:

N-(5-(2-((6-aminohexyl)(benzyl)amino)-1-hydroxyethyl)-2-(benzyloxy)phenyl)formamide trifluoroacetate

6-Chloropurine riboside

Downstream raw materials:

N-(2-hydroxy-5-(1-hydroxy-2-(6-(N₆-adenosinyl)hexylamino)ethyl)phenyl)formamide

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