2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

Base Information

Chemical Name:2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide
CAS No.:1383956-64-6
Molecular Formula:C₁₈H₂₂F₃N₃O₂
Molecular Weight:369.387
Hs Code.:

Synonyms:2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

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Chemical Property of 2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

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Technology Process of 2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

There total 2 articles about 2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383956-69-1
C₁₈H₂₀F₃N₃O₄

: 1383956-64-6
2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 80 ℃; for 16h;
DOI:10.1016/j.tetlet.2012.05.013

Reference yield:

: 931-53-3
Cyclohexyl isocyanide

: 109466-87-7
4-(trifluoromethyl)-2-nitrobenzaldehyde

: 1383956-64-6
2-oxo-9-trifluoromethyl-1,2,3,4,5,6-hexahydrobenzo[b][1,5]diazocine-6-carboxylic acid cyclohexylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol; water / 0.5 h / 20 °C

1.2: 20 h / 20 °C

2.1: iron; ammonium chloride / ethanol; water / 16 h / 80 °C

With iron; ammonium chloride; In ethanol; water; 1.1: Ugi condensation / 1.2: Ugi condensation;
DOI:10.1016/j.tetlet.2012.05.013