N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

Base Information

Chemical Name:N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide
CAS No.:171285-77-1
Molecular Formula:C₁₉H₂₃NO₃S₂
Molecular Weight:377.529
Hs Code.:

Synonyms:N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

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Chemical Property of N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

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Technology Process of N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

There total 8 articles about N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 171285-77-1
N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

Guidance literature:

Reference yield:

: 62404-59-5
4-(N-acetyl-N-methylamino)iodobenzene

: 161386-86-3
2-mercapto-4-[(2S)-2,2,4-trimethyl-1,3-dioxolan-4-yl]-thiophene

: 171285-77-1
N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

Guidance literature:: With copper(l) iodide; potassium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 2h; Yield given;
DOI:10.1021/jm00020a008

Reference yield:

: 2-Thiophen-3-yl-propane-1,2-diol

: 171285-77-1
N-methyl-4'-<<4-(2,2,4-trimethyl-1,3-dioxolan-4-yl)thien-2-yl>thio>acetanilide

Guidance literature:: Multi-step reaction with 4 steps

1: PTSA / acetone / 0.75 h / Heating

2: 1.) BuLi

3: NaSMe / dimethylformamide / 0.5 h / 130 °C

4: K₂CO₃, CuI / dimethylformamide / 2 h / 130 °C

With copper(l) iodide; n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; sodium thiomethoxide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00020a008