C₄₃H₇₄O₆Si₃

Base Information

Chemical Name:C₄₃H₇₄O₆Si₃
CAS No.:676254-80-1
Molecular Formula:C₄₃H₇₄O₆Si₃
Molecular Weight:771.313
Hs Code.:

C<sub>43</sub>H<sub>74</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₄₃H₇₄O₆Si₃

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Chemical Property of C₄₃H₇₄O₆Si₃

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Technology Process of C₄₃H₇₄O₆Si₃

There total 10 articles about C₄₃H₇₄O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 676254-79-8
(3R,4S,5S,8S,9S,10S)-11-(tert-Butyl-dimethyl-silanyloxy)-5,9-bis-methoxymethoxy-4,8,10-trimethyl-1-trimethylsilanyl-undec-1-yn-3-ol

: 676254-80-1
C₄₃H₇₄O₆Si₃

Guidance literature:: With 2-imidazoline; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2003.12.067

Reference yield:

: 104701-87-3
(2S)-3-(tert-butyl-dimethyl-silyloxy)-2-methyl-propanal

: 676254-80-1
C₄₃H₇₄O₆Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: 71 percent / Ph₃P; Et₂Zn / Pd(OAc)2

2.1: 92 percent / BuLi

3.1: 100 percent / Noyori (R,R)-ruthenium/p-cymene catalyst / propan-2-ol

4.1: 97 percent / H₂; Et₃N / Pd(OH)2 / 5171.62 Torr

5.1: 97 percent / H₂ / Pd/C / ethanol

6.1: 100 percent / Dess-Martin periodinane; NaHCO₃

7.2: 90 percent / Dess-Martin periodinane; NaHCO₃

8.1: 62 percent / Noyori (R,R)-ruthenium/p-cymene catalyst / propan-2-ol

9.1: 100 percent / imidazoline / dimethylformamide

With 2-imidazoline; n-butyllithium; ((1R,2R)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)ruthenium chloride(I) (4-cymene); p-cymene catalyst; hydrogen; diethylzinc; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; triphenylphosphine; palladium diacetate; palladium dihydroxide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol; 4.1: Noyori reaction / 8.1: Dess-Martin oxidation / 9.2: Dess-Martin oxidation / 10.1: Noyori reaction;
DOI:10.1016/j.tetlet.2003.12.067

Reference yield:

: 202119-27-5
(2S,3S,4S)-1-((tert-butyldimethylsilyl)oxy)-2,4-dimethylhex-5-yn-3-ol

: 676254-80-1
C₄₃H₇₄O₆Si₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: 92 percent / BuLi

2.1: 100 percent / Noyori (R,R)-ruthenium/p-cymene catalyst / propan-2-ol

3.1: 97 percent / H₂; Et₃N / Pd(OH)2 / 5171.62 Torr

4.1: 97 percent / H₂ / Pd/C / ethanol

5.1: 100 percent / Dess-Martin periodinane; NaHCO₃

6.2: 90 percent / Dess-Martin periodinane; NaHCO₃

7.1: 62 percent / Noyori (R,R)-ruthenium/p-cymene catalyst / propan-2-ol

8.1: 100 percent / imidazoline / dimethylformamide

With 2-imidazoline; n-butyllithium; ((1R,2R)-N-p-toluenesulfonyl-1,2-diphenylethylenediamine)ruthenium chloride(I) (4-cymene); p-cymene catalyst; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; palladium dihydroxide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; isopropyl alcohol; 3.1: Noyori reaction / 7.1: Dess-Martin oxidation / 8.2: Dess-Martin oxidation / 9.1: Noyori reaction;
DOI:10.1016/j.tetlet.2003.12.067