4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one

Base Information

• Chemical Name: 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one
• CAS No.: 1020667-77-9
• Molecular Formula: C₂₂H₂₂N₂O₇
• Molecular Weight: 426.426
• Mol file: 1020667-77-9.mol

Synonyms:4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one

Chemical Property of 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one

There total 2 articles about 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)imino]-4,9-dihydrofuro[3,4-b]quinolin-1(3H)-one (1020667-78-0) → 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one (1020667-77-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 4h; under 7500.75 Torr;

DOI:10.1021/jo800166b

Reference yield: 80.0%

4-methyl-6,7-(methylenedioxy)-1-oxo-9-[(3,4,5-trimethoxyphenyl)amino]-1,3-dihydrofuro[3,4-b]quinolin-4-ium trifluoromethanesulfonate (1020667-83-7) → 4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)amino]-3a,4-dihydrofuro[3,4-b]quinolin-1(3H)-one (1020667-77-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 10h;

DOI:10.1021/jo800166b

upstream raw materials:

4-methyl-6,7-(methylenedioxy)-1-oxo-9-[(3,4,5-trimethoxyphenyl)amino]-1,3-dihydrofuro[3,4-b]quinolin-4-ium trifluoromethanesulfonate

4-methyl-6,7-(methylenedioxy)-9-[(3,4,5-trimethoxyphenyl)imino]-4,9-dihydrofuro[3,4-b]quinolin-1(3H)-one