C₁₁H₇F₃O

Base Information

• Chemical Name: C₁₁H₇F₃O
• CAS No.: 913558-45-9
• Molecular Formula: C₁₁H₇F₃O
• Molecular Weight: 212.171
• Mol file: 913558-45-9.mol

Synonyms:C₁₁H₇F₃O

Chemical Property of C₁₁H₇F₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₇F₃O

There total 1 articles about C₁₁H₇F₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopent-2-enone (930-30-3) + (2,3,5- trifluorophenyl)boronic acid (247564-73-4) → C11H7F3O (913558-45-9)

Guidance literature:

With 2Cl^(1-)*H₃Sb⁽²⁺⁾; sodium acetate; palladium diacetate; acetic acid; for 18h; Inert atmosphere;

DOI:10.1016/j.bmcl.2010.06.041

Reference yield:

C11H7F3O (913558-45-9) + oxalic acid diethyl ester (95-92-1) → C15H11F3N2O2

Guidance literature:

C₁₁H₇F₃O; oxalic acid diethyl ester; With potassium tert-butylate; In ethanol; tert-butyl alcohol; for 1h;

With hydrazine hydrochloride; In ethanol; tert-butyl alcohol; for 15h;

Reference yield:

C11H7F3O (913558-45-9) → C13H9F3N6

Guidance literature:

Multi-step reaction with 5 steps

1.1: potassium tert-butylate / ethanol; tert-butyl alcohol / 1 h

1.2: 15 h

2.1: formic acid; ammonium formate / palladium on activated charcoal / ethanol; water / 12 h / 85 °C

3.1: ammonia / 1,4-dioxane; water / 12 h

4.1: triethylamine; trifluoroacetic anhydride / tetrahydrofuran / 2 h / -5 - 20 °C

5.1: sodium azide; zinc dibromide / water; isopropyl alcohol / 24 h / 85 °C

With formic acid; sodium azide; potassium tert-butylate; ammonia; ammonium formate; triethylamine; trifluoroacetic anhydride; zinc dibromide; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; ethanol; water; isopropyl alcohol; tert-butyl alcohol;

upstream raw materials:

cyclopent-2-enone

(2,3,5- trifluorophenyl)boronic acid