2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...

Base Information

• Chemical Name: 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...
• CAS No.: 142065-13-2
• Molecular Formula: C₆₆H₇₆N₆O₁₄
• Molecular Weight: 1177.36

Synonyms:2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...

Chemical Property of 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...

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Technology Process of 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent...

There total 3 articles about 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione (118715-67-6) + 4-(Methoxymethoxy)benzylamine (142039-75-6) → 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent... (142065-13-2)

Guidance literature:

With sodium carbonate; sodium iodide; In acetonitrile;

DOI:10.1021/jo9505583

Reference yield:

4-cyanophenol (767-00-0) → 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent... (142065-13-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 52 percent / Aliquat, NaOH / CH₂Cl₂; H₂O

2: 75 percent / LiAlH₄, sulfuric acid / tetrahydrofuran

3: 75 percent / Na₂CO₃, NaI / acetonitrile

With sodium hydroxide; lithium aluminium tetrahydride; Aliquat; sulfuric acid; sodium carbonate; sodium iodide; In tetrahydrofuran; dichloromethane; water; acetonitrile;

DOI:10.1021/jo9505583

Reference yield:

4-(Methoxymethoxy)-1-benzonitrile (161196-99-2) → 2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<4-(methoxymethoxy)phenylmethyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacyclopent... (142065-13-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / LiAlH₄, sulfuric acid / tetrahydrofuran

2: 75 percent / Na₂CO₃, NaI / acetonitrile

With lithium aluminium tetrahydride; sulfuric acid; sodium carbonate; sodium iodide; In tetrahydrofuran; acetonitrile;

DOI:10.1021/jo9505583

upstream raw materials:

5,7,12,13b,13c,14-hexahydro-1,4,8,11-tetrakis<2-(2-chloro-ethoxy)ethoxy>-13b,13c-diphenyl-6H,13H-5a,6a,12a,13a-tetraazabenz<5,6>azuleno<2,1,8-ija>benzazulene-6,13-dione

4-(Methoxymethoxy)benzylamine

4-cyanophenol

4-(Methoxymethoxy)-1-benzonitrile

Downstream raw materials:

2a,8,9,12,13,14,15,17,18,25,26,29,30,31,32,34,35,38b-octadecahydro-2a,38b-diphenyl-13,30-bis<<4-(diphenylphosphito)phenyl>methyl>-1H,4H-6,37:20,23-dietheno-2,22:3.21-dimethano-5H,11H,28H,38H-7,10,16,19,24,27,33,36-octaoxa-2,3,4a,13,30,38a-hexaazacycl...

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