C₃₁H₄₀O₃

Base Information

• Chemical Name: C₃₁H₄₀O₃
• CAS No.: 1326708-06-8
• Molecular Formula: C₃₁H₄₀O₃
• Molecular Weight: 460.657
• Mol file: 1326708-06-8.mol

Synonyms:C₃₁H₄₀O₃

Chemical Property of C₃₁H₄₀O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₄₀O₃

There total 1 articles about C₃₁H₄₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C31H38O3 (1326707-98-5) → C31H40O3 (1326708-06-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; toluene; for 24h; stereoselective reaction; Inert atmosphere; Reflux;

DOI:10.1021/ol2017966

Reference yield: 90.0%

C31H40O3 (1326708-06-8) + p-toluenesulfonyl chloride (98-59-9) → C38H46O5S (1326707-99-6)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol2017966

Reference yield:

C31H40O3 (1326708-06-8) → C38H45IO5S (1326708-00-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: iodine; sodium hydrogencarbonate / acetonitrile / 2.17 h / 0 °C / Inert atmosphere; Darkness

With dmap; iodine; sodium hydrogencarbonate; triethylamine; In dichloromethane; acetonitrile;

DOI:10.1021/ol2017966

upstream raw materials:

C₃₁H₃₈O₃

Downstream raw materials:

C₃₈H₄₅IO₅S

C₃₁H₃₉NO₂

C₃₈H₄₂BrNO₃

C₃₈H₄₆O₅S