C₁₄H₂₀BrN₃O₂

Base Information

Chemical Name:C₁₄H₂₀BrN₃O₂
CAS No.:1342259-46-4
Molecular Formula:C₁₄H₂₀BrN₃O₂
Molecular Weight:342.236
Hs Code.:

C<sub>14</sub>H<sub>20</sub>BrN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₄H₂₀BrN₃O₂

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Chemical Property of C₁₄H₂₀BrN₃O₂

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Technology Process of C₁₄H₂₀BrN₃O₂

There total 5 articles about C₁₄H₂₀BrN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1342259-45-3
3-azido-1-bromo-4-(4-tert-butoxyphenyl) butan-2-one

: 1342259-46-4
C₁₄H₂₀BrN₃O₂

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1002/asia.201100523

Reference yield:

: C₁₈H₂₅N₃O₅

: 1342259-46-4
C₁₄H₂₀BrN₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 0 °C / Inert atmosphere

2: hydrogen bromide / dichloromethane; water / 3 h / 0 °C / Inert atmosphere

3: sodium tetrahydroborate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; hydrogen bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1002/asia.201100523

Reference yield:

: 4727-00-8,18822-59-8,186698-58-8
O-t-Butyl-L-tyrosine

: 1342259-46-4
C₁₄H₂₀BrN₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: copper(ll) sulfate pentahydrate; triflic azide; potassium carbonate / methanol; dichloromethane; water / 20 °C / Inert atmosphere

2: 4-methyl-morpholine / tetrahydrofuran / 0.25 h / -40 °C / Inert atmosphere

3: diethyl ether / 0 °C / Inert atmosphere

4: hydrogen bromide / dichloromethane; water / 3 h / 0 °C / Inert atmosphere

5: sodium tetrahydroborate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; sodium tetrahydroborate; copper(ll) sulfate pentahydrate; triflic azide; hydrogen bromide; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/asia.201100523