Technology Process of C23H22N2O2
There total 6 articles about C23H22N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate;
In
water; N,N-dimethyl-formamide;
at 110 ℃;
for 0.333333h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2011.05.052
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / acetonitrile / 20 °C
2.1: sodium hydroxide
2.2: 20 °C
3.1: phosphorus pentoxide
4.1: potassium carbonate / acetonitrile / 8 h / Reflux
5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 8 h / 80 °C / Inert atmosphere
6.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / water; N,N-dimethyl-formamide / 0.33 h / 110 °C / Microwave irradiation
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; phosphorus pentoxide; potassium acetate; sodium carbonate; potassium carbonate; triethylamine; sodium hydroxide;
In
water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.052
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / N,N-dimethyl-formamide / 8 h / 80 °C / Inert atmosphere
2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sodium carbonate / water; N,N-dimethyl-formamide / 0.33 h / 110 °C / Microwave irradiation
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; sodium carbonate;
In
water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.052