7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Base Information

Chemical Name:7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride
CAS No.:102393-12-4
Molecular Formula:C₂₄H₃₆Cl₂O₂
Molecular Weight:427.455
Hs Code.:

Synonyms:7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Suppliers and Price of 7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

There total 15 articles about 7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3710-01-8
1,4-bis(2-carboxyethyl)-2,3,5,6-tetramethylbenzene

: 102393-12-4
7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Guidance literature:: Multi-step reaction with 13 steps

1: 89.4 percent / cc. H₂SO₄ / toluene

2: 89.6 percent / B₂H₆ / tetrahydrofuran

3: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

4: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

5: H₂O, KOH / Heating

6: 94.6 percent / quinoline / 0.33 h / Heating

7: 95 percent / cc. H₂SO₄ / toluene

8: 99 percent / B₂H₆ / tetrahydrofuran

9: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

10: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

11: H₂O, KOH / Heating

12: diethylformamide / Heating

13: SOCl₂ / Heating

With quinoline; potassium hydroxide; thionyl chloride; N-ethylpropionamide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;

Reference yield:

: 63134-94-1
1.4-Bis(2.2-bis-aethoxycarbonyl-aethyl)-2.3.5.6-tetramethyl-benzol

: 102393-12-4
7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Guidance literature:: Multi-step reaction with 15 steps

1: H₂O, KOH / Heating

2: 94.7 percent / quinoline / 0.33 h / Heating

3: 89.4 percent / cc. H₂SO₄ / toluene

4: 89.6 percent / B₂H₆ / tetrahydrofuran

5: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

6: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

7: H₂O, KOH / Heating

8: 94.6 percent / quinoline / 0.33 h / Heating

9: 95 percent / cc. H₂SO₄ / toluene

10: 99 percent / B₂H₆ / tetrahydrofuran

11: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

12: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

13: H₂O, KOH / Heating

14: diethylformamide / Heating

15: SOCl₂ / Heating

With quinoline; potassium hydroxide; thionyl chloride; N-ethylpropionamide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;

Reference yield:

: 118214-26-9
1,4-bis(3-hydroxypropyl)-2,3,5,6-tetramethylbenzene

: 102393-12-4
7-[4-(6-Chlorocarbonyl-hexyl)-2,3,5,6-tetramethyl-phenyl]-heptanoyl chloride

Guidance literature:: Multi-step reaction with 11 steps

1: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

2: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

3: H₂O, KOH / Heating

4: 94.6 percent / quinoline / 0.33 h / Heating

5: 95 percent / cc. H₂SO₄ / toluene

6: 99 percent / B₂H₆ / tetrahydrofuran

7: 86 percent / 48 percent HBr / H₂O / 0.5 h / Heating

8: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

9: H₂O, KOH / Heating

10: diethylformamide / Heating

11: SOCl₂ / Heating

With quinoline; potassium hydroxide; thionyl chloride; N-ethylpropionamide; sulfuric acid; water; hydrogen bromide; sodium; diborane; In tetrahydrofuran; water; toluene;