(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

Base Information

Chemical Name:(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2
CAS No.:95616-02-7
Molecular Formula:C₃₈H₃₈P₂S₂Ti
Molecular Weight:668.679
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>)2Ti(SCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

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Chemical Property of (C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

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Technology Process of (C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

There total 1 articles about (C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 3190-79-2
(2-mercaptoethyl)diphenylphosphine

: 95616-02-7
(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

: 95616-06-1
(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)Cl

Guidance literature:: With triethylamine; In benzene; byproducts: triethylamine hydrochloride; under N2, 2 equiv of Et3N was added dropwise with stirring to soln. of 1 equiv of Ti-complex in benzene with 2 equiv of ligand, stirred for 4 h; filtered, chromd. on alumina column, eluted with freshly distd. degassed benzene, solvent removed under vac., treated with hexane, solvent evapd.;

Reference yield: 60.0%

: 95616-02-7
(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2)2

: 95616-03-8
(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2CH₃)2⁽²⁺⁾*2I^(1-)=(C₅H₅)2Ti(SCH₂CH₂P(C₆H₅)2CH₃I)2

Guidance literature:: With methyl iodide; In tetrahydrofuran; under N2, 3 equiv of CH3I was added dropwise with stirring to 1 equiv of Ti-complex in freshly distd. degassed THF, stirred for 2 h; concd., volume reduiced, filtered, washed with THF; elem. anal.;