3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

Base Information

Chemical Name:3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride
CAS No.:915777-42-3
Molecular Formula:C₁₁H₁₆N₂O₅S*ClH
Molecular Weight:324.785
Hs Code.:

Synonyms:3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

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Chemical Property of 3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

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Technology Process of 3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

There total 3 articles about 3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83489-61-6
3-(ethyl(3-hydroxyphenyl)amino)propane-1-sulfonic acid

: 915777-42-3
3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

Guidance literature:: With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 3.16667h; Inert atmosphere;
DOI:10.1002/chem.200801104

Reference yield:

: 591-27-5
m-Hydroxyaniline

: 915777-42-3
3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

2: isopropyl alcohol / 3 h / Reflux; Inert atmosphere

3: sodium nitrite; hydrogenchloride / water / 1.5 h / 0 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In water; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/acs.joc.9b03217

Reference yield:

: 621-31-8
3-(ethylamino)phenol

: 915777-42-3
3-(ethyl(3-hydroxy-4-nitrosophenyl)amino)propane-1-sulfonic acid hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol / 3 h / Reflux; Inert atmosphere

2: sodium nitrite; hydrogenchloride / water / 1.5 h / 0 °C

With hydrogenchloride; sodium nitrite; In water; isopropyl alcohol;
DOI:10.1021/acs.joc.9b03217