6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione]

Base Information

• Chemical Name: 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione]
• CAS No.: 1298131-01-7
• Molecular Formula: C₁₉H₂₁N₇O₆
• Molecular Weight: 443.419
• Mol file: 1298131-01-7.mol

Synonyms:6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione]

Chemical Property of 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione]

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione]

There total 2 articles about 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

6-Amino-1,3-dimethylbarbituric acid (6642-31-5) + 3-nitro-benzaldehyde (99-61-6) → 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione] (1298131-01-7)

Guidance literature:

With N,N,N′,N′-tetramethylethylenediaminium bis-hydrogensulfate; In neat (no solvent); at 120 ℃; for 0.333333h;

DOI:10.1007/s11164-019-04036-3

Reference yield: 54.0%

6-Amino-1,3-dimethylbarbituric acid (6642-31-5) + 1-((3-nitrophenyl)(pyrrolidin-1-yl)methyl)naphthalen-2-ol (1334232-93-7) → 6,6'-diamino-1,1',3,3'-tetramethyl-5,5'-(3-nitrobenzylidene)bis[pyrimidine-2,4(1H,3H)-dione] (1298131-01-7)

Guidance literature:

With p-toluenesulfonic acid monohydrate; In acetonitrile; at 100 ℃; for 0.133333h; Microwave irradiation;

DOI:10.1080/00397911.2016.1239740

upstream raw materials:

6-Amino-1,3-dimethylbarbituric acid

3-nitro-benzaldehyde

1-((3-nitrophenyl)(pyrrolidin-1-yl)methyl)naphthalen-2-ol