(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

Base Information

Chemical Name:(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2
CAS No.:199740-20-0
Molecular Formula:C₆₄H₄₈F₁₀P₂PdPt
Molecular Weight:1370.52
Hs Code.:

Synonyms:(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

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Chemical Property of (diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

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Technology Process of (diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

There total 3 articles about (diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: cis-[Pd(pentafluorophenyl)2(THF)2]

: 199740-15-3
cis-bis(phenylacetylide)bis(diphenyl(tert-butylethynyl)phosphine)platinum

: 199740-20-0
(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

Guidance literature:: In dichloromethane; N2-atmosphere; equimolar amts., stirring for 15 min at room temp.; concn., crystn. on addn. of hexane and standing at -30°C; elem. anal.;
DOI:10.1021/om970663y

Reference yield: 40.0%

: cis-[Pd(pentafluorophenyl)2(THF)2]

: 199740-15-3
cis-bis(phenylacetylide)bis(diphenyl(tert-butylethynyl)phosphine)platinum

: 199740-20-0
(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

: 199740-30-2
(diphenyl(tert-butylethynyl)phosphine)2Pt(μ3-η(2)-phenylacetylide)2(Pd(pentafluorophenyl)2)2

Guidance literature:: In dichloromethane; N2-atmosphere; 2 equivs. of Pd(C6F5)2(THF)2; evapn., extn. (hexane), recrystn. (CH2Cl2:hexane, -30°C); elem. anal.;
DOI:10.1021/om970663y

Reference yield:

: cis-[Pd(pentafluorophenyl)2(THF)2]

: 199740-15-3
cis-bis(phenylacetylide)bis(diphenyl(tert-butylethynyl)phosphine)platinum

: 199740-20-0
(diphenyl(tert-butylethynyl)phosphine)2Pt(μ-η(1):η(2)-phenylacetylide)2Pd(pentafluorophenyl)2

: 199740-30-2
(diphenyl(tert-butylethynyl)phosphine)2Pt(μ3-η(2)-phenylacetylide)2(Pd(pentafluorophenyl)2)2

: 7440-05-3
palladium

Guidance literature:: In dichloromethane; byproducts: decafluorobiphenyl; N2-atmosphere; 2 equivs. of Pd(C6F5)2(THF)2, standing for 12 h; not sepd.; NMR spectroscopy;
DOI:10.1021/om970663y