Technology Process of (η5-((3,5-dichlorobenzyl)oxy)divinylborane)(η5-cyclopentadienyl)cobalt
There total 1 articles about (η5-((3,5-dichlorobenzyl)oxy)divinylborane)(η5-cyclopentadienyl)cobalt which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
diethyl ether;
byproducts: pyridine*HCl; Under N2, dropwise addn. of a soln. of 3,5-dichlorobenzyl alcohol and pyridine in ether to a stirred soln. of Co-complex in ether at room temp., stirring for 5 min., ppt. of pyridine*HCl forms.; Filtn. through alumina, concg. under vac., addn. of hexane, cooling to -78°C, filtn., elem. anal.;