cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

Base Information

Chemical Name:cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆
CAS No.:84117-39-5
Molecular Formula:C₄₃H₃₂ClN₂OOsP₂*F₆P
Molecular Weight:1025.3
Hs Code.:

cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF<sub>6</sub>

Synonyms:cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

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Chemical Property of cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

Chemical Property:

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Technology Process of cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

There total 1 articles about cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89689-84-9
[Os(1,10-phenanthroline)Cl₄]

: 13991-08-7
o-phenylenebis(diphenylphosphine)

: 84117-39-5
cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

Guidance literature:: With carbon monoxide; In ethylene glycol; Complex was allowed to react with phosphine at reflux in ethylene glycol under an atm. of CO;;
DOI:10.1021/om00086a016

Reference yield: 75.0%

: 84117-39-5
cis-{Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl}PF₆

: 84117-29-3
Os(C₁₂H₈N₂)((C₆H₅)2PC₆H₄P(C₆H₅)2)(P(C₆H₅)3)H⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: With triphenylphosphine; In ethylene glycol; byproducts: HCOCH2OH, CO, HCl; A soln. of complex in ethylene glycol was heated at reflux with PPh3;; chromy.;;
DOI:10.1021/om00086a016

Reference yield:

: 84117-39-5
[Os(1,10-phenanthroline)(1,2-bis(diphenylphosphino)benzene)(CO)Cl]PF₆

: 84117-29-3
Os(C₁₂H₈N₂)((C₆H₅)2PC₆H₄P(C₆H₅)2)(P(C₆H₅)3)H⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: With ethylene glycol; triphenylphosphine; In ethylene glycol; excess PPh3 in ethylene glycol, reflux; purified by chromy. (Al2O3, toluene-MeCN);