C₁₁H₆Br₂Cl₂N₂O

Base Information

• Chemical Name: C₁₁H₆Br₂Cl₂N₂O
• CAS No.: 1428422-88-1
• Molecular Formula: C₁₁H₆Br₂Cl₂N₂O
• Molecular Weight: 412.895
• Mol file: 1428422-88-1.mol

Synonyms:C₁₁H₆Br₂Cl₂N₂O

Chemical Property of C₁₁H₆Br₂Cl₂N₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₆Br₂Cl₂N₂O

There total 1 articles about C₁₁H₆Br₂Cl₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,6-trichloropyridazine (6082-66-2) + 3,5-dibromo-4-hydroxytoluene (2432-14-6) → C11H6Br2Cl2N2O (1428422-88-1)

Guidance literature:

3,5-dibromo-4-hydroxytoluene; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h; Cooling with ice;

3,4,6-trichloropyridazine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2012.12.049

Reference yield:

C11H6Br2Cl2N2O (1428422-88-1) + 4-Aminobenzonitrile (873-74-5) → C18H11Br2ClN4O (1403768-66-0)

Guidance literature:

C₁₁H₆Br₂Cl₂N₂O; 4-Aminobenzonitrile; With hydrogenchloride; In ethanol; water; Reflux;

With sodium hydroxide; In ethanol; water; pH=8; Cooling;

DOI:10.1016/j.bmc.2012.12.049

Reference yield:

C11H6Br2Cl2N2O (1428422-88-1) → C18H12Br2N4O2 (1403768-79-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: hydrogenchloride / water; ethanol / Reflux

1.2: pH 8 / Cooling

2.1: acetic acid / Reflux

2.2: pH 8 / Cooling

With hydrogenchloride; acetic acid; In ethanol; water;

DOI:10.1016/j.bmc.2012.12.049

upstream raw materials:

3,4,6-trichloropyridazine

3,5-dibromo-4-hydroxytoluene

Downstream raw materials:

C₁₈H₁₂Br₂N₄O₂

C₁₈H₁₁Br₂ClN₄O