triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

Base Information

Chemical Name:triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate
CAS No.:1231951-13-5
Molecular Formula:C₂₇H₃₅IN₂O₆
Molecular Weight:610.489
Hs Code.:

Synonyms:triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

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Chemical Property of triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

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Technology Process of triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

There total 1 articles about triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6279-86-3
methanetricarboxylic acid triethyl ester

: 1231951-12-4
1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-ol

: 1231951-13-5
triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; trimethylphosphane; In 2-methyltetrahydrofuran; toluene; at -78 - 20 ℃; for 2.86667h; Inert atmosphere;

Reference yield:

: 1231951-13-5
triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate

: 64-19-7,77671-22-8
acetic acid

: [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]acetic acid acetate

Guidance literature:: triethyl [1-[(3-iodophenyl)methyl]-2-(1-methylethyl)-4,5,6,7-tetrahydro-1H-benzimidazol-7-yl]methanetricarboxylate; With sodium hydroxide; In methanol; water; at 80 ℃; for 17h; Inert atmosphere;

acetic acid; at 80 ℃; for 24h; Inert atmosphere;