5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

Base Information

Chemical Name:5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde
CAS No.:177755-43-0
Molecular Formula:C₁₇H₁₃FN₂OS
Molecular Weight:312.367
Hs Code.:

Synonyms:5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

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Chemical Property of 5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

Chemical Property:

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Technology Process of 5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

There total 5 articles about 5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

dimethylformamide [DMF]: dimethylformamide [DMF]

: tetramethylethylenediamine (TMEDA)

: 177755-42-9
5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1-(1-methyl-1-ethoxymethyl)-1H-imidazole

: 177755-43-0
5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

Guidance literature:: With hydrogenchloride; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; hexane;

Reference yield:

: 1-(4-fluorophenyl)-2-(methylsulfonylphenyl)-ethane-1-one

: 177755-43-0
5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / acetic acid

2: sodium hydrogencarbonate / methanol; water; toluene

3: sodium hydroxide / toluene

4: hydrogenchloride; sodium hydrogencarbonate / tetrahydrofuran; ethanol; hexane

With hydrogenchloride; sodium hydroxide; bromine; sodium hydrogencarbonate; In tetrahydrofuran; methanol; ethanol; hexane; water; acetic acid; toluene;

Reference yield:

: 177755-38-3
5-(4-Fluorophenyl)-4-(4-methylthiophenyl)-2-trifluoromethyl-1H-imidazole

: 177755-43-0
5-(4-fluorophenyl)-4-(4-methylthiophenyl)-1H-imidazole-2-carboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; water; ethyl acetate

2: sodium hydroxide / toluene

3: hydrogenchloride; sodium hydrogencarbonate / tetrahydrofuran; ethanol; hexane

With hydrogenchloride; sodium hydroxide; sodium hydrogencarbonate; In tetrahydrofuran; methanol; ethanol; hexane; water; ethyl acetate; toluene;