(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

Base Information

Chemical Name:(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime
CAS No.:83258-76-8
Molecular Formula:C₃₄H₃₅NO₆
Molecular Weight:553.655
Hs Code.:

Synonyms:(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

Suppliers and Price of (3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

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Technology Process of (3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

There total 5 articles about (3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 86496-30-2
(2S,3R,4R,5R)-2,3,4,6-tetrakis(benzyloxy)-5-hydroxyhexanal oxime

: 83258-76-8
(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

Guidance literature:: With sodium periodate; sodium acetate; In ethanol; water; at 60 ℃;
DOI:10.3390/molecules16119495

Reference yield:

: 84799-77-9
methyl 2,3,4,6-tetra-O-benzyl-D-glucopyranoside

: 83258-76-8
(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; acetic acid / 90 °C

2: ethanol; hydroxylamine hydrochloride; sodium / 74 °C

3: sodium periodate; sodium acetate / ethanol; water / 60 °C

With sodium periodate; ethanol; sulfuric acid; hydroxylamine hydrochloride; sodium acetate; sodium; acetic acid; In ethanol; water;
DOI:10.3390/molecules16119495

Reference yield:

: 100-44-7
benzyl chloride

: 83258-76-8
(3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-one oxime

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / 120 °C

2: sulfuric acid; acetic acid / 90 °C

3: ethanol; hydroxylamine hydrochloride; sodium / 74 °C

4: sodium periodate; sodium acetate / ethanol; water / 60 °C

With sodium periodate; ethanol; sulfuric acid; hydroxylamine hydrochloride; sodium acetate; sodium; sodium hydride; acetic acid; In ethanol; water;
DOI:10.3390/molecules16119495