methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

Base Information

Chemical Name:methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside
CAS No.:142886-55-3
Molecular Formula:C₂₁H₂₄O₁₀
Molecular Weight:436.416
Hs Code.:

Synonyms:methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

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Technology Process of methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

There total 6 articles about methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 53901-95-4,108608-06-6,58523-18-5
p-acetoxycinnamoyl chloride

: 108586-51-2
methyl 2,3-di-O-acetyl-α-L-arabinofuranoside

: 142886-55-3
methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

Guidance literature:: With pyridine; for 5h;
DOI:10.1016/S0008-6215(00)90492-0

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 142886-55-3
methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / 4 h

2: 80 percent / SOCl₂ / benzene / 0.75 h / Heating

3: 84 percent / pyridine / 5 h

With pyridine; thionyl chloride; In benzene;
DOI:10.1016/S0008-6215(00)90492-0

Reference yield:

: 27542-85-4
4-acetoxycinnamic acid

: 142886-55-3
methyl 2,3-di-O-acetyl-5-O-(4'-O-acetyl-p-coumaroyl)-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / SOCl₂ / benzene / 0.75 h / Heating

2: 84 percent / pyridine / 5 h

With pyridine; thionyl chloride; In benzene;
DOI:10.1016/S0008-6215(00)90492-0