(2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II)

Base Information

• Chemical Name: (2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II)
• CAS No.: 942472-16-4
• Molecular Formula: C₇₆H₈₈N₄O₄Pd
• Molecular Weight: 1227.98
• Mol file: 942472-16-4.mol

Synonyms:(2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II)

Chemical Property of (2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II)

There total 1 articles about (2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)porphyrin-2,3,12,13-tetraone + palladium dichloride → (2,3,12,13-tetraoxo-5,10,15,20-tetrakis(3,5-di-tert-butylphenyl)chlorinato)palladium(II) (942472-16-4)

Guidance literature:

With sodium acetate; In acetic acid; toluene; soln. of tetraone, PdCl2, and AcONa in toluene/glacial acetic acid heated at reflux for 5 min; CH2Cl2 added, org. phase sepd., washed with water, aq. Na2CO3, and water, dried over Na2SO4, filtered, filtrate evapd. to dryness, column chromy. (silica, CH2Cl2/light petroleum 1:1);

DOI:10.1021/ja070759b