(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

Base Information

Chemical Name:(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride
CAS No.:123294-75-7
Molecular Formula:C₁₆H₂₁ClO₃
Molecular Weight:296.794
Hs Code.:

Synonyms:(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

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Chemical Property of (E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

Chemical Property:

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Technology Process of (E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

There total 1 articles about (E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123294-74-6
(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoic acid

: 123294-75-7
(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

Guidance literature:: DOI:10.1246/cl.1989.465

Reference yield:

: 123294-75-7
(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

: 53101-49-8,53174-06-4,53188-07-1,56305-04-5
(S)-6-hydroxy-2,5,7,8-tetramethylchroman-2-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

2: NBS, t-BuOK / -20 deg C, 2 h, RT, 2 h

3: Bu₃SnH / benzene / 10 h / 90 °C

4: 98 percent / cc. HCl / 10 h / Heating

With hydrogenchloride; N-Bromosuccinimide; potassium tert-butylate; tri-n-butyl-tin hydride; In benzene;
DOI:10.1246/cl.1989.465

Reference yield:

: 123294-75-7
(E)-4-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-2-methyl-but-2-enoyl chloride

: 123294-78-0
(3S,8aR)-3-[2-(2,5-Dimethoxy-3,4,6-trimethyl-phenyl)-ethyl]-3-methyl-tetrahydro-pyrrolo[2,1-c][1,4]oxazine-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

2: NBS, t-BuOK / -20 deg C, 2 h, RT, 2 h

3: Bu₃SnH / benzene / 10 h / 90 °C

With N-Bromosuccinimide; potassium tert-butylate; tri-n-butyl-tin hydride; In benzene;
DOI:10.1246/cl.1989.465