Technology Process of 2-iodo-6-nitrobenzaldehyde
There total 5 articles about 2-iodo-6-nitrobenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide;
In
benzene;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Trimethyl borate; dimethylsulfide borane complex / tetrahydrofuran / 6 h / Inert atmosphere; Reflux
2: silica gel; dipyridinium dichromate / dichloromethane / 6 h / 20 °C / Inert atmosphere
With
dipyridinium dichromate; Trimethyl borate; dimethylsulfide borane complex; silica gel;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.7b03577
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C / Inert atmosphere
1.2: 1.5 h / 90 °C / Inert atmosphere
2.1: Trimethyl borate; dimethylsulfide borane complex / tetrahydrofuran / 6 h / Inert atmosphere; Reflux
3.1: silica gel; dipyridinium dichromate / dichloromethane / 6 h / 20 °C / Inert atmosphere
With
hydrogenchloride; dipyridinium dichromate; Trimethyl borate; dimethylsulfide borane complex; silica gel; sodium nitrite;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/acs.orglett.7b03577
