(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

Base Information

Chemical Name:(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone
CAS No.:130675-46-6
Molecular Formula:C₁₅H₁₉NO₆
Molecular Weight:309.319
Hs Code.:

Synonyms:(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

Chemical Property:

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Technology Process of (4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

There total 3 articles about (4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130675-45-5
(4S)-4-<(methoxymethoxy)methyl>-2-oxazolidinone

: 5437-45-6
Benzyl bromoacetate

: 130675-46-6
(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; for 20h; Ambient temperature;
DOI:10.1248/cpb.38.1601

Reference yield:

: 95407-06-0
N-(benzyloxycarbonyl)-O-(methoxymethyl)-L-serinol

: 130675-46-6
(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) H₂, 2) K₂CO₃ / 1) 5percent Pd-C / 1) EtOH, 2) 130 to 140 deg C, 30 min

2: 96 percent / NaH / tetrahydrofuran; dimethylformamide / 20 h / Ambient temperature

With hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.1601

Reference yield:

: 95407-05-9
N-(benzyloxycarbonyl)-O-(methoxymethyl)-L-serine methyl ester

: 130675-46-6
(4S)-3-<(benzyloxycarbonyl)methyl>-4-<(methoxymethoxy)methyl>-2-oxazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / NaBH₄ / ethanol / 3 h / Ambient temperature

2: 1) H₂, 2) K₂CO₃ / 1) 5percent Pd-C / 1) EtOH, 2) 130 to 140 deg C, 30 min

3: 96 percent / NaH / tetrahydrofuran; dimethylformamide / 20 h / Ambient temperature

With sodium tetrahydroborate; hydrogen; sodium hydride; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.1601