4-methoxybenzoylsulfenyl bromide

Base Information

• Chemical Name: 4-methoxybenzoylsulfenyl bromide
• CAS No.: 85156-92-9
• Molecular Formula: C₈H₇BrO₂S
• Molecular Weight: 247.112

Synonyms:4-methoxybenzoylsulfenyl bromide

Chemical Property of 4-methoxybenzoylsulfenyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methoxybenzoylsulfenyl bromide

There total 3 articles about 4-methoxybenzoylsulfenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

CH3OC6H4COSHgC6H5 (79293-00-8) → 4-methoxybenzoylsulfenyl bromide (85156-92-9)

Guidance literature:

With N-Bromosuccinimide; In chloroform; for 0.5h; Ambient temperature;

DOI:10.1055/s-1982-30042

Reference yield: 40.0%

Silver; 4-methoxy-benzenecarbothioate (87662-84-8) → 4-methoxybenzoylsulfenyl bromide (85156-92-9)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1055/s-1983-30420

Reference yield:

Diphenyltin bis<4-methoxythiobenzoate> (88584-82-1) → 4-methoxybenzoylsulfenyl bromide (85156-92-9)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; chloroform; at 0 ℃; for 0.5h;

DOI:10.1055/s-1983-30525

upstream raw materials:

CH₃OC₆H₄COSHgC₆H₅

Silver; 4-methoxy-benzenecarbothioate

Diphenyltin bis<4-methoxythiobenzoate>

Downstream raw materials:

p-tolylselenyl bromide

C₁₅H₁₄O₂SSe

Phenylselenyl bromide

Se-phenyl (4-methoxyphenyl)-oxomethanesulfenoselenoate

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