C₄₈H₄₈O₇

Base Information

Chemical Name:C₄₈H₄₈O₇
CAS No.:1413373-48-4
Molecular Formula:C₄₈H₄₈O₇
Molecular Weight:736.905
Hs Code.:

C<sub>48</sub>H<sub>48</sub>O<sub>7</sub>

Synonyms:C₄₈H₄₈O₇

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Chemical Property of C₄₈H₄₈O₇

Chemical Property:

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Technology Process of C₄₈H₄₈O₇

There total 11 articles about C₄₈H₄₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1413373-46-2
C₄₈H₄₆O₆

: 1413373-48-4
C₄₈H₄₈O₇

Guidance literature:: C₄₈H₄₆O₆; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-48-4
C₄₈H₄₈O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C

With pyridine; oxalyl dichloride; tributylphosphine; dimethylsulfide borane complex; L-Selectride; dimethyl sulfoxide; L-proline; 1,1'-azodicarbonyl-dipiperidine; trichlorophosphate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 6.1: Mitsunobu reaction;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413373-48-4
C₄₈H₄₈O₇

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: L-Selectride / tetrahydrofuran / 18 h / 0 - 20 °C / Inert atmosphere

5.2: 0.25 h

6.1: 1,1'-azodicarbonyl-dipiperidine; tributylphosphine / toluene / 0.5 h / 0 °C / Inert atmosphere

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 3 h / 0 - 20 °C

With sodium tetrahydroborate; n-butyllithium; tributylphosphine; dimethylsulfide borane complex; L-Selectride; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; 1,1'-azodicarbonyl-dipiperidine; 18-crown-6 ether; In tetrahydrofuran; hexane; dichloromethane; toluene; 6.1: Mitsunobu reaction;