C₅₁H₅₃N₇O₅

Base Information

Chemical Name:C₅₁H₅₃N₇O₅
CAS No.:1369595-32-3
Molecular Formula:C₅₁H₅₃N₇O₅
Molecular Weight:844.026
Hs Code.:

C<sub>51</sub>H<sub>53</sub>N<sub>7</sub>O<sub>5</sub>

Synonyms:C₅₁H₅₃N₇O₅

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Chemical Property of C₅₁H₅₃N₇O₅

Chemical Property:

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Technology Process of C₅₁H₅₃N₇O₅

There total 11 articles about C₅₁H₅₃N₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1369595-29-8
C₄₅H₄₈ClN₇O₅

: 98-80-6
phenylboronic acid

: 1369595-32-3
C₅₁H₅₃N₇O₅

Guidance literature:: With potassium carbonate; XPhos; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In 1,4-dioxane; water; at 110 ℃; for 22h;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-32-3
C₅₁H₅₃N₇O₅

Guidance literature:: Multi-step reaction with 6 steps

1: acetic acid / ethanol / 6 h / Reflux

2: polyphosphoric acid / 2 h / 80 °C

3: caesium carbonate / dimethyl sulfoxide / 18 h / 90 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 1.5 h / 90 °C

5: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 18 h / 90 °C

6: potassium carbonate; XPhos / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / 1,4-dioxane; water / 22 h / 110 °C

With potassium acetate; potassium carbonate; caesium carbonate; acetic acid; XPhos; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1369595-32-3
C₅₁H₅₃N₇O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonia / methanol / 0.5 h / 20 - 30 °C

1.2: 16 h / 20 - 60 °C

2.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

3.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 18 h / 90 °C

4.1: potassium carbonate; XPhos / tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex / 1,4-dioxane; water / 22 h / 110 °C

With N-Bromosuccinimide; ammonia; potassium carbonate; XPhos; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane; water;