potassium bis-(2-methoxyethyl)dithiocarbamate

Base Information

Chemical Name:potassium bis-(2-methoxyethyl)dithiocarbamate
CAS No.:1144472-82-1
Molecular Formula:C₇H₁₄NO₂S₂*K
Molecular Weight:247.424
Hs Code.:

Synonyms:potassium bis-(2-methoxyethyl)dithiocarbamate

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Chemical Property of potassium bis-(2-methoxyethyl)dithiocarbamate

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Technology Process of potassium bis-(2-methoxyethyl)dithiocarbamate

There total 1 articles about potassium bis-(2-methoxyethyl)dithiocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-15-0,12122-00-8
carbon disulfide

: 111-95-5
Bis-(2-methoxyethyl)amine

: 1144472-82-1
potassium bis-(2-methoxyethyl)dithiocarbamate

Guidance literature:: With potassium hydroxide; In acetone; for 3.5h;
DOI:10.1039/a707650i

Reference yield: 95.0%

: [Ru(CHCHtBu)Cl(CO)(BTD)(PPh₃)₂]

: 1144472-82-1
potassium bis-(2-methoxyethyl)dithiocarbamate

: 1228538-06-4
[Ru(CHCHtBu)(CO)(S₂CN(CH₂CH₂OMe)2)(triphenylphosphine)2]

Guidance literature:: In water; acetone; addn. of aq. soln. of dithiocarbamate salt to acetone soln. of rutheniumcompd., stirring for 1 h; concg., isolation of ppt., washing with water, ethanol and petroleum ether, drying in vac., elem. anal.;
DOI:10.1039/b925536b

Reference yield: 87.0%

: ammonium hexafluorophosphate

: cis-[RuCl₂(dppm)2]

: 1144472-82-1
potassium bis-(2-methoxyethyl)dithiocarbamate

: [Ru(S₂CN(CH₂CH₂OMe)2)(bis(diphenylphosphino)methane)2](hexafluorophosphate)

Guidance literature:: In methanol; dichloromethane; addn. of methanolic soln. of dithiocarbamate salt and NH4PF6 to CH2Cl2 soln. of ruthenium compd., stirring for 30 min; evapn., dissolving in CH2Cl2, filtration through celite, addn. of ethanol, concg., isolation of ppt., washing with ethanol and petroleum ether,drying in vac., elem. anal.;
DOI:10.1039/b925536b