3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

Base Information

Chemical Name:3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole
CAS No.:172795-45-8
Molecular Formula:C₃₃H₂₈Cl₂N₂O₄
Molecular Weight:587.502
Hs Code.:

Synonyms:3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

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Chemical Property of 3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

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Technology Process of 3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

There total 3 articles about 3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 151290-21-0
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole

: 870193-26-3
3-(4-chlorophenyl)-7-hydroxymethyl-4,6-dimethoxyindole

: bis(3-(4'-chlorophenyl)-4,6-dimethoxyindol-7-yl)methane

: 3-(4-chlorophenyl)-4,6-dimethoxy-2,7-bis[3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl]indole

: 172795-45-8
3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

Guidance literature:: With acetic acid; for 0.166667h; Heating;
DOI:10.1016/j.tet.2005.08.075

Reference yield:

: 151290-21-0
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole

: 172795-45-8
3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphorus oxychloride / 0 °C

1.2: 84 percent / sodium hydroxide / H₂O; dimethylformamide

2.1: 98 percent / sodium borohydride / tetrahydrofuran / 12 h / Heating

3.1: 33 percent / acetic acid / 0.17 h / Heating

With sodium tetrahydroborate; acetic acid; trichlorophosphate; In tetrahydrofuran; 1.1: Vilsmeier formylation;
DOI:10.1016/j.tet.2005.08.075

Reference yield:

: 362590-16-7
3-(4-chlorophenyl)-4,6-dimethoxy-1H-indole-7-carbaldehyde

: 172795-45-8
3-(4-chlorophenyl)-4,6-dimethoxy-2-(3-(4-chlorophenyl)-4,6-dimethoxyindol-7-ylmethyl)indole

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium borohydride / tetrahydrofuran / 12 h / Heating

2: 33 percent / acetic acid / 0.17 h / Heating

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.tet.2005.08.075